Başlık için Kimya Bölümü listeleme
Toplam kayıt 209, listelenen: 137-156
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Self-assembly of an organocatalyst for the enantioselective synthesis of Michael adducts and α-aminoxy alcohols in a nonpolar medium
(2013)A proline-thiourea host-guest complex is described as a self-assembled organocatalyst for the enantioselective Michael addition of aldehydes to nitroolefins and for the asymmetric ?-aminoxylation of both aldehydes and ... -
A sensitive and selective RP-LC method for the simultaneous determination of the antihypertensive drugs, enalapril, lercanidipine, nitrendipine and their validation
(2013)A RP-LC method is presented, which is sensitive and selective for the simultaneous determination of enalapril-lercanidipine and enalapril-nitrendipine binary mixtures in their pharmaceutical dosage forms. The analyte peaks ... -
Separation and elution order of the enantiomers of some beta-agonists using polysaccharide-based chiral columns and normal phase eluents by high-performance liquid chromatography
(Elsevier B.V., 2016)In this study separation of enantiomers of 8 chiral ?-agonists were studied on 6 polysaccharide-based chiral columns in polar-organic and alcohol-hydrocarbon mobile phases. No separation of enantiomers was observed on any ... -
A simple and rapid method for preparing carbon nanopore electrode ensemble by coating a glassy carbon electrode with chromate
(Hitit University, 2016)A simple preparation method for carbon nanopore electrode ensemble (CNEE) was reported. The CNEE consists of a number of pinholes which remain after coating a carbon surface with chromate. The transformation from transient ... -
Simple and sensitive adsorptive stripping voltammetric assay of granisetron from its dosage form by platinum nanoparticles modified electrodes
(Elsevier B.V., 2017)Base to the interfacial adsorptive nature of granisetron (GRN) on platinum particles modified glassy carbon electrode (PtPs/GCE). A sensitive analytical method for trace analysis of GRN based on the adsorptive stripping ... -
A simple flow injection spectrophotometric procedure for direct determination of copper(II) in environmental samples
(Chemical Publishing Co., 2014)A new simple, rapid and sensitive flow-injection spectrophotometric detection method has been developed for the on-line determination of copper(II) in environmental water samples. The method is based on the measurement of ... -
Simple, sensitive and reliable LC-DAD method of gemifloxacin determination in pharmaceutical dosage forms
(2012)A sensitive, accurate, rapid, fully validated, reliable and easy method was developed for the quantification of gemifloxacin mesylate (GEM) using liquid chromatography (LC) with DAD detection. In this method; a reversed-phase ... -
Simultaneous determination and validation of emtricitabine, rilpivirine and tenofovir from biological samples using LC and CE methods
(John Wiley and Sons Ltd, 2018)A combination of antiretroviral agents is frequently used in effective treatment of the human immunodeficiency virus infection. In this study, two different separation methods are presented for the simultaneous determination ... -
Simultaneous determination and validation of some binary mixtures of antihypertensive drugs using ratio derivative spectrophotometric method
(Maik Nauka Publishing / Springer SBM, 2014)Ratio derivative spectrophotometric technique is presented for the rapid, accurate and precise simultaneous determination of olmesartan medoxomil (OLM), hydrochlorothiazide (HCT), and zofenopril (ZOF) as well as HCT binary ... -
Simultaneous determination of amlodipine besylate and rosuvastatin calcium in binary mixtures by voltammetric and chromatographic techniques
(Institute for Ionics, 2016)Voltammetric and liquid chromatographic (LC) methods have been developed for the simultaneous determination of amlodipine besylate (AML) and rosuvastatin calcium (ROS) for the first time. Detailed electrochemical behavior ... -
Simultaneous determination of three phenolic compounds in water samples by pre-column derivatization coupled with reversed-phase high performance liquid chromatography
(Hacettepe University, 2018)In this study, a sensitive and accurate method for simultaneous separation and determination of three phenolic compounds (phenol, m-cresol and resorcinol) in water by revesed-phase high performance liquid chromatography ... -
Simultaneous estimation and validation of some binary mixtures of antihypertensive drugs by RP-LC methods using two new generation silica columns
(Elsevier B.V., 2013)Two reversed phase liquid chromatographic (RP-LC) techniques are presented for the rapid, accurate, precise, simultaneous determination of olmesartan-hydrochlorothiazide and zofenopril-hydrochlorothiazide binary mixtures ... -
Simultaneous estimation of ceftazidime and ceftizoxime in pharmaceutical formulations by HPLC method
(2011)The aim of the present study was to develop a fast, sensitive and reliable method for rapid screening of cephalosporin injectable dosage forms namely ceftazidime and ceftizoxime to the detection of counterfeit and substandard ... -
Solvent effect on endosulfan adsorption onto polymeric arginine-methacrylate cryogels
(Springer Verlag, 2018)Endosulfan is a persistent insecticide that is still used in some countries even though it is life-threatening and banned in the agricultural struggle. The solubility of pesticides in water is negligible. It is known that ... -
Solvent effects on pKa values of some substituted sulfonamides in acetonitrile-water binary mixtures by the UV-spectroscopy method
(2009)The examination of the dissociation constants of sulfonamides is essential in drug-design studies and in explaining the biopharmaceutical properties of substances. The dissociation constants of ten common human and veterinary ... -
Spectrophotometric determination of acidity constants of some macrolides in acetonitrile-water binary mixtures
(2010)The acidity constants of eight macrolides (erythromycin, roxithromycin, oleandomycin, azithromycin, josamycin, tylosin tartrate, tilmicosin and spiramycin) have been determined in acetonitrile-water binary mixtures (30%, ... -
Spectrophotometric determination of acidity constants of some novel methotrexate-like compounds in water and acetonitrile-water binary mixtures
(2010)The acidity constants of four novel methotrexate like compounds (NPALA; (N-[4-[[2-hydroxy -1-naphtyl)methylene]amino]benzoyl-?-alanin) TPALA; (N-[4-(2-thiophene-aldiminobenzoyl)-?-alanin), SAL-ALA; N-[4-[[2-hydroxyphenyl ... -
Spectroscopic and thermal properties of newly mixed azocalix[4]arene ester derivatives
(Elsevier B.V., 2014)The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene ... -
Spectroscopic properties of 2,2’-[Thiobis(p-phenylenenitrilo-methylidyne)]bis(4-chloro/bromo/methyl/nitro/methoxy)phenol
(Hacettepe University, 2012)Novel Schiff base has been synthesized from the reaction of 4,4’-diaminodiphenyl sulfide with 2-hydroxy5-substituebenzaldehyde and 2-hydroxynaphtaldehyde. The compounds were characterized by elemental analysis, FT-IR, 1 H ... -
Spectroscopic, antiproliferative and antiradical properties of Cu(II), Ni(II), and Zn(II) complexes with amino acid based Schiff bases
(Birkhauser Boston, 2014)Novel six Cu(II), Ni(II), and Zn(II) complexes with Schiff bases derived from 4-aminobenzoic acid with terephtaldehyde and amino acids (glycine, ?-alanine). Structures have been proposed from elemental analysis, UV-Vis, ...