Yayın tarihi için Kimya Bölümü listeleme
Toplam kayıt 209, listelenen: 61-80
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Fully validated simultaneous determination of bisoprolol fumarate and hydrochlorothiazide in their dosage forms using different voltammetric, chromatographic, and spectrophotometric analytical methods
(2013)Voltammetric, chromatographic, and spectrophotometric methods were developed for the simultaneous determination of bisoprolol fumarate (BIS) and hydrochlorothiazide (HCZ). Differential pulse and square wave voltammetry ... -
A validated stability-indicating RP-LC method for the simultaneous determination of amlodipine and perindopril in tablet dosage form and their stress degradation behavior under ICH-recommended stress conditions
(2013)A stability-indicating RP-LC assay method was developed for the simultaneous determination of the cardiovascular drugs amlodipine and perindopril in the presence of degradation products generated from forced decomposition ... -
Determination of pKa values of some butyrophenones, their sensitive LC-UV analysis in pharmaceutical dosage forms and stress degradation behavior under ICH-recommended stress conditions
(2013)In this study, pKa values of some ionizable butyrophenones, namely, benperidol, droperidol, and haloperidol were determined using by the dependence of the retention factor on pH of the mobile phase. The effect of the mobile ... -
Platinized carbon nanoelectrodes as potentiometric and amperometric SECM probes
(2013)Micrometer-sized platinized carbon electrodes have previously been used for the detection of reactive oxygen and nitrogen species (ROS and RNS) in biological systems. Here, we report the preparation and characterization ... -
Fabrication, characterization, and chemical etching of Ag nanoelectrodes
(2013)The previously developed methodologies for fabricating flat, polished nanoelectrodes were extended to produce silver electrodes with the radii from 50 nm to micrometers. The prepared electrodes were characterized by ... -
Electroanalytical characterization of levodropropizine and its voltammetric determination in pharmaceuticals
(2013)Levodropropizine is a cough suppressant and easily oxidizable at the carbon-base electrodes. The electrooxidative behavior and determination of levodropropizine on glassy carbon and boron-doped diamond electrodes were ... -
Ethyl 2-[(2-hydroxybenzylidene)amino]-6-methyl-4,5,6,7-tetrahydrothieno[2, 3-c]pyridine-3-carboxylate
(2013)The title compound, C18H20N2O3S, exists as the phenol–imine form in the crystal and there are bifurcated intramolecular O—H…(N/O) hydrogen bonds present. The conformation about the C N bond is anti (1E); the C N imine bond ... -
Synthesis of a bipyridine-derived achiral thiourea trifluoromethanesulfonic acid salt and its application as an additive in organocatalytic asymmetric reactions
(2013)The host-guest complex of a proline-thiourea bipyridine trifluoromethanesulfonic acid salt can catalyze organocatalytic asymmetric reactions such as aldol, Michael, and Mannich in polar protic medium with high stereoselectivities. ... -
Electrochemical approach for the sensitive determination of anticancer drug epirubicin in pharmaceuticals in the presence of anionic surfactant
(Editions de l'Academie Republique Populaire, 2013)In this research, sensitive, rapid, different electrochemical methods were developed for the determination of anticancer drug epirubicin. The aim of the study was to fully validated determination of epirubicin in ... -
Validated electroanalytical and RP-LC assay of ertapenem in its pharmaceutical dosage form
(Editions de l'Academie Republique Populaire, 2013)Ertapenem is a member of carbapenem group beta-lactam antibiotics. The electrochemical behavior of ertapenem at the surface on a boron-doped diamond electrode is described. It is investigated and determined using cyclic, ... -
Inhibition effect of berberine on the corrosion of copper in acidic medium
(Editions de l'Academie Republique Populaire, 2013)Inhibition of copper corrosion by berberine in 0.5 M HCl was investigated by electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization techniques. The inhibition efficiency of berberine was studied for ... -
Analytical application of polymethylene blue-multiwalled carbon nanotubes modified glassy carbon electrode on anticancer drug irinotecan and determination of its ionization constant value
(Elsevier B.V., 2013)The voltammetric behavior of anticancer drug irinotecan (IRT) was investigated at poly (methylene blue)/multi-walled carbon nanotube (PMB/MWCNT) modified glassy carbon electrode (GCE). The modified electrode surface was ... -
Determination of dissociation constants of some antifungal drugs by two different methods at 298 K
(2013)The dissociation constants of eight antifungal drugs (fenticonazole, isoconazole, itraconazole, ketoconazole, miconazole, ornidazole, tinidazole, tioconazole) have been determined in water and acetonitrile-water binary ... -
Simultaneous estimation and validation of some binary mixtures of antihypertensive drugs by RP-LC methods using two new generation silica columns
(Elsevier B.V., 2013)Two reversed phase liquid chromatographic (RP-LC) techniques are presented for the rapid, accurate, precise, simultaneous determination of olmesartan-hydrochlorothiazide and zofenopril-hydrochlorothiazide binary mixtures ... -
A sensitive and selective RP-LC method for the simultaneous determination of the antihypertensive drugs, enalapril, lercanidipine, nitrendipine and their validation
(2013)A RP-LC method is presented, which is sensitive and selective for the simultaneous determination of enalapril-lercanidipine and enalapril-nitrendipine binary mixtures in their pharmaceutical dosage forms. The analyte peaks ... -
Synthesis, spectral characterisation and thermal behaviours of some new p-tert-butylcalix[4]arene and calix[4]arene-esters containing acryloyl groups
(2013)The mono-, di-, tri-, and tetra-acryloyl esters of p-tert-butylcalix [4]arene and calix[4]arene were synthesised by reacting acryloyl chloride with sodium salts of p-tert-butylcalix[4]arene and calix[4]arene in THF. The ... -
Preparation and Characterization of PVA/PVP Nanofibers as Promising Materials for Wound Dressing
(2013)The PVA/PVP, PVA/PVP with 5% and 10% chitosan and PVA/PVP-Iodine fibers were produced via electrospinning technique. Their morphological and chemical characteristics were examined with SEM, TGA, FT-IR, viscometer and ... -
Investigation of applicability of plant extracts (Euphorbia orientalis L.) instead of chemical disinfectants
(Wiley-Blackwell, 2013)[Abstract Not Available] -
Bazı metal organik kafes yapılı bileşiklerin hidrojen depolama performanslarının incelenmesi
(2013)Hidrojenin bilinen depolama sistemlerinden farklı olarak depolama ortamlarında kimyasal olarak veya zayıf van der Waals etkileşimleriyle fiziksel olarak tutunabildiği bilinmektedir. Hidrojen, fiziksel adsorpsiyonla karbon ... -
Study of structure and spectral characteristics of the Zinc(II) and Copper(II) complexes with 5,5-dimethyl-2-(2-(3-nitrophenyl) hydrazono)cyclohexane-1,3-dione and their effects on optical properties and the developing of the energy band gap and ınvestigation of antibacterial activity
(Sociedad Quimica de Mexico A.C., 2014)A new chelating ligand, 5,5-dimethyl-2-(2-(3-nitrophenyl) hydrazono)cyclohexane-1,3-dione (L), and four transition metal complexes were synthesized. The ligand and its complexes were characterized by IR, 1H and 13C-NMR ...