Konu "[Belirlenecek]" için Kimya Bölümü listeleme
Toplam kayıt 26, listelenen: 1-20
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4-[2-(2,2-Dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)hydrazin-1-yl] benzo-nitrile
(2010)In the title compound, C 13H 11N 3O 4, the dioxane ring adopts an envelope conformation with the C atom bonded to the dimethyl group in the flap position [deviation = 0.613 (1) Å]. The nitrile group and the attached benzene ... -
Bis(4-methoxybenzoato)-κ2O,O′;κO- bis(nicotinamide-κN1)zinc(II)
(2010)The asymmetric unit of the title complex, [Zn(C8H 7O3)2(C6H6N 2O)2], contains three crystallographically independent molecules with similar configurations. The ZnII cation is coordinated by two N atoms of two nicotinamide ... -
Bis(isonicotinamide-κN1)bis(4-methylbenzoato-κO) copper(II) dihydrate
(2010)In the centrosymmetric title compound, [Cu(C8H7O 2)2(C6H6N2O) 2]·2H2O, the CuII ion is located on a crystallographic inversion center. The asymmetric unit is completed by one 4-methylbenzoate anion, one isonicotinamide ... -
Design of pyrazolo-pyrrolo-pyrazines and pyrazolo-pyrrolo-diazepines via AuCl3-catalyzed and NaH-supported cyclization of N -propargyl pyrazoles
(American Chemical Society, 2015)A concise synthetic methodology for new heterocyclic scaffolds, such as pyrazolo-pyrrolo-pyrazine and pyrazolo-pyrrolo-diazepine skeletons, was developed. The key features of this method include (i) synthesis of pyrrole-derived ... -
Determination of dissociation constants of folinic acid (leucovorin), 5-fluorouracil, and irinotecan in hydro-organic media by a spectrophotometry method
(2010)In this study, a multiwavelength spectrophotometry method was used for the determination of the dissociation constants of drugs used for treatment of colorectal cancer, folinic acid (leucovorin), 5-fluorouracil, and ... -
Determination of pKa values of some antipsychotic drugs by HPLC-correlations with the kamlet and taft solvatochromic parameters and HPLC analysis in dosage forms
(2013)In this study, ionization constant (pKa) values were determined by using the dependence of the retention factor on the pH of the mobile phase for four ionizable drugs, namely, risperidone (RI), clozapine (CL), olanzapine ... -
Diaquabis(2-bromobenzoato-κO)bis(N,N diethylnicotinamide- κN1)cobalt(II)
(2010)In the mononuclear title compound, [Co(C7H4BrO 2)2(C10H14N2O) 2(H2O)2], the CoII ion is located on a crystallographic inversion center. The asymmetric unit is completed by one 2-bromobenzoate anion, one diethylnicotinamide ... -
DNA binding and cleavage activities of Na[B(Glu)(OH)2] ·2H2O, Na[B(Cit)(OH)2]·2H2O, Li[B(Sal)(OH)2], and Mg[B(Sal)(OH)2]·2H 2O complexes
(2013)The interaction of some previously reported complexes Na[B(Glu)(OH) 2]·2H2O, Na[B(Cit)(OH)2]·2H 2O, Li[B(Sal)(OH)2], and Mg[B(Sal)(OH)2] ·2H2O with cattle genomic DNA (CG-DNA) was investigated using UV absorption, viscosity ... -
Electrochemical approach for the sensitive determination of anticancer drug epirubicin in pharmaceuticals in the presence of anionic surfactant
(Editions de l'Academie Republique Populaire, 2013)In this research, sensitive, rapid, different electrochemical methods were developed for the determination of anticancer drug epirubicin. The aim of the study was to fully validated determination of epirubicin in ... -
Ethyl 2-[(2-hydroxybenzylidene)amino]-6-methyl-4,5,6,7-tetrahydrothieno[2, 3-c]pyridine-3-carboxylate
(2013)The title compound, C18H20N2O3S, exists as the phenol–imine form in the crystal and there are bifurcated intramolecular O—H…(N/O) hydrogen bonds present. The conformation about the C N bond is anti (1E); the C N imine bond ... -
Fully validated simultaneous determination of bisoprolol fumarate and hydrochlorothiazide in their dosage forms using different voltammetric, chromatographic, and spectrophotometric analytical methods
(2013)Voltammetric, chromatographic, and spectrophotometric methods were developed for the simultaneous determination of bisoprolol fumarate (BIS) and hydrochlorothiazide (HCZ). Differential pulse and square wave voltammetry ... -
Inhibition effect of berberine on the corrosion of copper in acidic medium
(Editions de l'Academie Republique Populaire, 2013)Inhibition of copper corrosion by berberine in 0.5 M HCl was investigated by electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization techniques. The inhibition efficiency of berberine was studied for ... -
Intramolecular Gold-Catalyzed and NaH-Supported Cyclization Reactions of N-Propargyl Indole Derivatives with Pyrazole and Pyrrole Rings: Synthesis of Pyrazolodiazepinoindole, Pyrazolopyrazinoindole, and Pyrrolopyrazinoindole
(American Chemical Society, 2015)Gold-catalyzed and NaH-supported intramolecular cyclization of N-propargyl indole derivatives with pyrazole and pyrrole units attached to indole is described. An efficient route to the synthesis of pyrazolodiazepinoindole, ... -
Investigation of immobilization and kinetic properties of catalase enzyme on poly(HEMA-GMA) cryogel
(Slovak Academy of Sciences Institute of Experimental Physics Department of Biophysics, 2017)Catalase is a metalloenzyme, which is found in almost all aerobic respiratory organisms. This enzyme acts as a detoxification agent for the hydrogen peroxide (H2O2) compound, protecting tissues and cells from oxidative ... -
Investigation of voltammetric behavior and electroanalytical determination of anticancer epirubicin via glassy carbon electrode using differential pulse and square wave voltammetry techniques
(Editions de l'Academie Republique Populaire, 2015)The electrochemical oxidation of epirubicin was investigated using cyclic, differential pulse and square wave voltammetry at glassy carbon electrode. The aim of the study was to determine epirubicin levels in pharmaceuticals ... -
Magnetic nanocomposites of boron and Vitamin C
(Royal Society of Chemistry, 2017)Magnetic nanocomposites comprising elemental boron and vitamin C in the form of mono or bis(ascorbatoborate) complexes have been synthesized for targeted delivery/therapy applications. These nanocomposites were characterized ... -
PdAg-decorated three-dimensional reduced graphene oxide-multi-walled carbon nanotube hierarchical nanostructures for high-performance hydrogen peroxide sensing
(Cambridge University Press, 2018)High-performance electrochemical hydrogen peroxide (H2O2) sensors based on PdAg nanoparticle-decorated reduced graphene oxide (rGO) and multi-walled carbon nanotube (MWCNT) hybrids were developed. The nanostructures were ... -
Polarographic investigation of dienogest
(Electrochemical Society Inc., 2018)Dienogest (DGN), is an orally administered synthetic progestin that has shown to have selective progesterone receptor (PR) agonistic activity and oral progestational potency on endometrium. In this paper, the investigation ... -
Selective and sensitive determination of repaglinide in pharmaceuticals by voltammetric and LC methods
(Editions de l'Academie Republique Populaire, 2015)Detailed electrochemical study and novel voltammetric and LC methods are presented for the determination of repaglinide (RPG) in pharmaceuticals. Repaglinide in methanol: buffer solution (20:80; v/v) shows one or two anodic ... -
Self-assembly of an organocatalyst for the enantioselective synthesis of Michael adducts and α-aminoxy alcohols in a nonpolar medium
(2013)A proline-thiourea host-guest complex is described as a self-assembled organocatalyst for the enantioselective Michael addition of aldehydes to nitroolefins and for the asymmetric ?-aminoxylation of both aldehydes and ...