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Toplam kayıt 194, listelenen: 173-192
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Synthesis, characterization, conformational equilibrium and intramolecular hydrogen bond analysis of Novel Azocalix[4]arenes including acryloyl moiety using DFT studies
(Elsevier B.V., 2019)Azocalix[4]arenes were synthesized via diazo-coupling reaction with aniline in 1:1, 1:2, 1:3 and 1:4 molar ratio. Novel Azocalix[4]arenes having Acryloyl moiety were prepared esterification reaction with metallic sodium ... -
Synthesis, spectral characterisation and thermal behaviours of some new p-tert-butylcalix[4]arene and calix[4]arene-esters containing acryloyl groups
(2013)The mono-, di-, tri-, and tetra-acryloyl esters of p-tert-butylcalix [4]arene and calix[4]arene were synthesised by reacting acryloyl chloride with sodium salts of p-tert-butylcalix[4]arene and calix[4]arene in THF. The ... -
Synthesis, spectral, and thermal studies of Co(II), Ni(II), Cu(II), and Zn(II)-glycinato complexes and ınvestigation of their biological properties: Crystal structure of [Cu(µ-gly)2(H2O)]n
(Taylor and Francis Inc., 2016)The complexes of metal cations with glycine amino acid were synthesized and characterized by FTIR, TGA, UV-Vis, and elemental analysis methods. Just the CuII-complex was suitably obtained as a single crystal. Neighboring ... -
Synthesis, spectral, thermal studies of Co(II), Ni(II), Cu(II) and Zn(II)-arginato Complexes. crystal structure of monoaquabis(arginato‐κO,κN)copper(II). [Cu(arg)2(H2O)].NaNO3
(Chinese Chemical Society Taiwan, 2014)Transition metal complexes of arginine (using Co(II), Ni(II), Cu(II) and Zn(II) cations separately) were synthesized and characterized by FTIR, TG/DTA-DrTG, UV-Vis spectroscopy and elemental analysis methods. Cu(II)-Arg ... -
Synthesis, spectroscopic and thermal characterization of non-metal cation (nmc) pentaborates salts containing cations derived from histidine and arginine
(Hacettepe University, 2012)The new non-metal cation (NMC) pentaborate structures of cationic histidine and arginine aminoacids were synthesized and characterized using spectroscopic (11B NMR and IR) methods. Their thermal properties have been ... -
Synthesis, structural characterization and biological activities of metal(II) complexes with Schiff bases derived from 5-bromosalicylaldehyde: Ru(II) complexes transfer hydrogenation
(Elsevier B.V., 2019)In this study, two novel Schiff base ligands (L1 and L2) derived from condensation of methyl 2-amino-6-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylate and methyl 2-amino-6-phenyl-4,5,6,7-tetrahydrobenzo[b]th ... -
Synthesis, structural characterization and biological activity of novel cyclohexane-1,3-dione ligands and their metal complexes
(MDPI AG, 2015)Some new Zn(II) and Cu(II) complexes [Cu(L1)(OAc)2]·H2O, [Cu(L1)(NO3)H2O]·NO3·3.5H2O, [Zn(L1)(NO3)2]·4.5H2O, [Zn(L1)(OAc)2(H2O)2]·3H2O, [Cu2(L2)(OAc)4]·2H2O·2DMF, [Cu(L2)2]·2NO3·1.5DMF·H2O, [Zn(L2)2(NO3)2]·DMF and ... -
Synthesis, structural, spectroscopic characterization, and structural comparison of 3-hydroxybenzoate and nicotinamide/N,N-diethylnicotinamide mixed ligand complexes with Zn(II)
(Kluwer Academic Publishers, 2012)The mixed-ligand 3-hydroxybenzoic acid complex of Zn(II) with nicotinamide and N,N-diethylnicotinamide were synthesized and characterized (colorless single crystals, [Zn(3-hba) 2 (H 2 O) 2 (na) 2 ] and [Zn(3-hba) 2 (H 2 ... -
Synthetic routes to manganese oxoborate and correlations between experimental parameters and properties
(Elsevier Sci Ltd, 2021)This study examines manganese oxoborate synthesis in three different routes and the role of process parameters on structure and morphology of the products. Borax or boric acid and simple manganese salts were used as raw ... -
Tetraaquabis(orotato-O)cobalt(II) dihydrate
(2010)In the title CoII complex, [Co(C5H3N 2O4)2(H2O)4]·2H2O, the CoII ion is located on an inversion center and is coordinated by two orotate (2,6-dioxo-1,2,3,6-tetrahydropyrimidine-4-carboxylate) anions and four water mol-ecules ... -
Therapeutic Effects of Newly Synthesized Boron Compounds (BGM and BGD) on Hepatocellular Carcinoma
(Humana Press Inc, 2021)Boron has an important potential for facilitating biological activity and for use in pharmaceutical drug design. Boron glycine monoester (BGM) and boron glycine diester (BGD) compounds containing boron atoms were synthesized ... -
Two novel mixed-ligand zinc-acesulfame compounds: Synthesis, spectroscopic and thermal characterization and biological applications
(Elsevier B.V., 2020)Two new tetrahedral acesulfame complexes, acesulfamato(N)acesulfamato(O)bis(3-aminopyridine) zinc(II) (C18H20N6O8S2Zn, Zn-ace-3ap) and bis(acesulfamato-O)bis(benzotriazole)zinc(II) (C20H18N8O8S2Zn, Zn-ace-bta), were ... -
Use of amino acid-based polymeric material for isolation of a protein from poison
(Elsevier B.V., 2017)Melittin is a small protein with 126 amino acid residues which exists in the bee and snake venom. In this study, the Fe(II)-Ni(II) double-salt incorporated poly(2-hydroxyethyl methacrylate-N-methacryloyl-L-aspartic acid), ... -
Use of nicotinamide decorated polymeric cryogels as heavy metal sweeper
(Springer Verlag, 2018)Cryogels are synthetic polymers used in adsorption experiments in recent years. Because of their macropores, they provide an excellent advantage as an adsorbent in continuous and batch adsorption processes. In this study, ... -
A validated RP-HPLC method for the estimation of ornidazole in pharmaceutical dosage forms
(Hacettepe University, 2012)A new, simple, rapid, selective, precise and accurate isocratic reverse phase high performance liquid chromatography assay has been developed and validated for assay of Ornidazole in tablet formulations. Tinidazole was ... -
A validated RP-LC method for salmeterol and fluticasone in their binary mixtures and their stress degradation behavior under ICH-recommended stress conditions
(Maik Nauka Publishing / Springer SBM, 2014)Simple, accurate, precise and fully validated analytical methods for the simultaneous determination of salmeterol xinafoate and fluticasone propionate in combined dosage forms have been developed. These drugs were exposed ... -
A validated stability-indicating RP-LC method for the simultaneous determination of amlodipine and perindopril in tablet dosage form and their stress degradation behavior under ICH-recommended stress conditions
(2013)A stability-indicating RP-LC assay method was developed for the simultaneous determination of the cardiovascular drugs amlodipine and perindopril in the presence of degradation products generated from forced decomposition ... -
Voltammetric and RP-LC assay for determination of benidipine HCl
(2012)The detailed electrooxidative behavior of benidipine (BEN) has been studied by using glassy carbon (GC) and boron-doped diamond (BDD) electrodes. Using cyclic voltammetry, depending on the pH values and the working electrodes, ... -
Voltammetric and RP-LC assay for the antidepressant drug mirtazapine: A validated method for the pharmaceutical dosage form
(2013)In the present paper, rapid, sensitive, selective, accurate and precise analytical methodologies were developed for the determination of the antidepressant drug mirtazapine (MIR) using voltammetry and liquid chromatography. ... -
Voltammetric behavior and determination of antidepressant drug paroxetine at carbon-based electrodes
(Institute for Ionics, 2015)Simple, rapid, sensitive, and reproducible methods were developed for the assay of paroxetine in tablets. The electrooxidative behavior and determination of paroxetine on boron-doped diamond and edge plane graphite electrodes ...