Konu "[Belirlenecek]" için Makale Koleksiyonu listeleme
Toplam kayıt 21, listelenen: 1-20
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4-[2-(2,2-Dimethyl-4,6-dioxo-1,3-dioxan-5-ylidene)hydrazin-1-yl] benzo-nitrile
(2010)In the title compound, C 13H 11N 3O 4, the dioxane ring adopts an envelope conformation with the C atom bonded to the dimethyl group in the flap position [deviation = 0.613 (1) Å]. The nitrile group and the attached benzene ... -
Bis(4-methoxybenzoato)-κ2O,O′;κO- bis(nicotinamide-κN1)zinc(II)
(2010)The asymmetric unit of the title complex, [Zn(C8H 7O3)2(C6H6N 2O)2], contains three crystallographically independent molecules with similar configurations. The ZnII cation is coordinated by two N atoms of two nicotinamide ... -
Bis(isonicotinamide-κN1)bis(4-methylbenzoato-κO) copper(II) dihydrate
(2010)In the centrosymmetric title compound, [Cu(C8H7O 2)2(C6H6N2O) 2]·2H2O, the CuII ion is located on a crystallographic inversion center. The asymmetric unit is completed by one 4-methylbenzoate anion, one isonicotinamide ... -
Design of pyrazolo-pyrrolo-pyrazines and pyrazolo-pyrrolo-diazepines via AuCl3-catalyzed and NaH-supported cyclization of N -propargyl pyrazoles
(American Chemical Society, 2015)A concise synthetic methodology for new heterocyclic scaffolds, such as pyrazolo-pyrrolo-pyrazine and pyrazolo-pyrrolo-diazepine skeletons, was developed. The key features of this method include (i) synthesis of pyrrole-derived ... -
Determination of dissociation constants of folinic acid (leucovorin), 5-fluorouracil, and irinotecan in hydro-organic media by a spectrophotometry method
(2010)In this study, a multiwavelength spectrophotometry method was used for the determination of the dissociation constants of drugs used for treatment of colorectal cancer, folinic acid (leucovorin), 5-fluorouracil, and ... -
Determination of pKa values of some antipsychotic drugs by HPLC-correlations with the kamlet and taft solvatochromic parameters and HPLC analysis in dosage forms
(2013)In this study, ionization constant (pKa) values were determined by using the dependence of the retention factor on the pH of the mobile phase for four ionizable drugs, namely, risperidone (RI), clozapine (CL), olanzapine ... -
Diaquabis(2-bromobenzoato-κO)bis(N,N diethylnicotinamide- κN1)cobalt(II)
(2010)In the mononuclear title compound, [Co(C7H4BrO 2)2(C10H14N2O) 2(H2O)2], the CoII ion is located on a crystallographic inversion center. The asymmetric unit is completed by one 2-bromobenzoate anion, one diethylnicotinamide ... -
DNA binding and cleavage activities of Na[B(Glu)(OH)2] ·2H2O, Na[B(Cit)(OH)2]·2H2O, Li[B(Sal)(OH)2], and Mg[B(Sal)(OH)2]·2H 2O complexes
(2013)The interaction of some previously reported complexes Na[B(Glu)(OH) 2]·2H2O, Na[B(Cit)(OH)2]·2H 2O, Li[B(Sal)(OH)2], and Mg[B(Sal)(OH)2] ·2H2O with cattle genomic DNA (CG-DNA) was investigated using UV absorption, viscosity ... -
Ethyl 2-[(2-hydroxybenzylidene)amino]-6-methyl-4,5,6,7-tetrahydrothieno[2, 3-c]pyridine-3-carboxylate
(2013)The title compound, C18H20N2O3S, exists as the phenol–imine form in the crystal and there are bifurcated intramolecular O—H…(N/O) hydrogen bonds present. The conformation about the C N bond is anti (1E); the C N imine bond ... -
Fully validated simultaneous determination of bisoprolol fumarate and hydrochlorothiazide in their dosage forms using different voltammetric, chromatographic, and spectrophotometric analytical methods
(2013)Voltammetric, chromatographic, and spectrophotometric methods were developed for the simultaneous determination of bisoprolol fumarate (BIS) and hydrochlorothiazide (HCZ). Differential pulse and square wave voltammetry ... -
Intramolecular Gold-Catalyzed and NaH-Supported Cyclization Reactions of N-Propargyl Indole Derivatives with Pyrazole and Pyrrole Rings: Synthesis of Pyrazolodiazepinoindole, Pyrazolopyrazinoindole, and Pyrrolopyrazinoindole
(American Chemical Society, 2015)Gold-catalyzed and NaH-supported intramolecular cyclization of N-propargyl indole derivatives with pyrazole and pyrrole units attached to indole is described. An efficient route to the synthesis of pyrazolodiazepinoindole, ... -
Investigation of voltammetric behavior and electroanalytical determination of anticancer epirubicin via glassy carbon electrode using differential pulse and square wave voltammetry techniques
(Editions de l'Academie Republique Populaire, 2015)The electrochemical oxidation of epirubicin was investigated using cyclic, differential pulse and square wave voltammetry at glassy carbon electrode. The aim of the study was to determine epirubicin levels in pharmaceuticals ... -
Magnetic nanocomposites of boron and Vitamin C
(Royal Society of Chemistry, 2017)Magnetic nanocomposites comprising elemental boron and vitamin C in the form of mono or bis(ascorbatoborate) complexes have been synthesized for targeted delivery/therapy applications. These nanocomposites were characterized ... -
PdAg-decorated three-dimensional reduced graphene oxide-multi-walled carbon nanotube hierarchical nanostructures for high-performance hydrogen peroxide sensing
(Cambridge University Press, 2018)High-performance electrochemical hydrogen peroxide (H2O2) sensors based on PdAg nanoparticle-decorated reduced graphene oxide (rGO) and multi-walled carbon nanotube (MWCNT) hybrids were developed. The nanostructures were ... -
Polarographic investigation of dienogest
(Electrochemical Society Inc., 2018)Dienogest (DGN), is an orally administered synthetic progestin that has shown to have selective progesterone receptor (PR) agonistic activity and oral progestational potency on endometrium. In this paper, the investigation ... -
Self-assembly of an organocatalyst for the enantioselective synthesis of Michael adducts and α-aminoxy alcohols in a nonpolar medium
(2013)A proline-thiourea host-guest complex is described as a self-assembled organocatalyst for the enantioselective Michael addition of aldehydes to nitroolefins and for the asymmetric ?-aminoxylation of both aldehydes and ... -
Solvent effects on pKa values of some substituted sulfonamides in acetonitrile-water binary mixtures by the UV-spectroscopy method
(2009)The examination of the dissociation constants of sulfonamides is essential in drug-design studies and in explaining the biopharmaceutical properties of substances. The dissociation constants of ten common human and veterinary ... -
Study of asymmetric aldol and Mannich reactions catalyzed by proline-thiourea host-guest complexes in nonpolar solvents
(2013)A proline-thiourea host-guest complex has been described as a good catalyst for asymmetric reactions such as aldol and Mannich reactions. High stereoselectivities were obtained under optimal conditions. Thiourea was observed ... -
Synthesis, characterization of poly-2- (2-hydroxybenzylideneamino)-6- phenyl-4,5,6, 7-tetrahydrobenzo[b]thiophene-3-carbonitrile: Investigation of antibacterial activity and optical properties
(2012)The oxidative polycondensation reaction conditions of 2-(2- hydroxybenzylideneamino)-6-phenyl-4,5,6,7-tetrahydrobenzo[b]thiophene-3- carbonitrile were examined. The magnitude of the reflectance of the polymer decreases ... -
Tetraaquabis(orotato-O)cobalt(II) dihydrate
(2010)In the title CoII complex, [Co(C5H3N 2O4)2(H2O)4]·2H2O, the CoII ion is located on an inversion center and is coordinated by two orotate (2,6-dioxo-1,2,3,6-tetrahydropyrimidine-4-carboxylate) anions and four water mol-ecules ...