Synthesis, characterization and electrochemical performance of Nb doped LiFePO4/C cathodes by mechanochemical activation

dc.authorid0000-0001-9931-0778
dc.authorid0000-0002-0081-1642
dc.contributor.authorBağcı, Cengiz
dc.contributor.authorAkyıldız, Öncü
dc.date.accessioned2019-04-13T09:34:18Z
dc.date.available2019-04-13T09:34:18Z
dc.date.issued2018
dc.departmentHitit Üniversitesi, Mühendislik Fakültesi, Metalurji ve Malzeme Mühendisliği Bölümü
dc.description.abstractWe synthesized Nb-doped LiFePO4/C nano composite cathode materials by mechanochemical activation followed by a single step calcination. The starting chemicals of Li2CO3, FeC2O4.2H2O, NH4H2.PO4 and C6H8O7 as lithium, iron, phosphate, and carbon sources are mixed in a high energy ball mill (250 rpm, 5h) and calcined at 650 °C and 10 hours. The resultant materials are structurally (XRD, SEM, TEM) and electrochemically characterized and high purity LiFePO4 with high electrochemical performance is obtained. Voltage vs. specific capacity, discharge capacity vs. cycle number in manufactured battery is presented. An initial specific discharge capacity of 153 mAhg?1 and a specific discharge capacity of 128.4 mAhg?1 after the 8th charge/discharge cycling at 1C is recorded.
dc.description.provenanceSubmitted by Öncü Akyıldız (oncuakyildiz@hitit.edu.tr) on 2019-04-09T10:05:17Z No. of bitstreams: 1 document (47).pdf: 1584863 bytes, checksum: 661667b8f2d8278af61c1f0e95ac3966 (MD5)en
dc.description.provenanceApproved for entry into archive by Fatma Özdemir (fatmaozdemir@hitit.edu.tr) on 2019-04-13T09:34:18Z (GMT) No. of bitstreams: 1 document (47).pdf: 1584863 bytes, checksum: 661667b8f2d8278af61c1f0e95ac3966 (MD5)en
dc.description.provenanceMade available in DSpace on 2019-04-13T09:34:18Z (GMT). No. of bitstreams: 1 document (47).pdf: 1584863 bytes, checksum: 661667b8f2d8278af61c1f0e95ac3966 (MD5) Previous issue date: 2018-03-28en
dc.identifier.citationBağcı, C., Akyıldız, Ö. (2018). Synthesis, characterization and electrochemical performance of Nb doped LiFePO4/C cathodes by mechanochemical activation. Hittite Journal of Science and Engineering, 5(1), 49-55.
dc.identifier.doi10.17350/HJSE19030000077
dc.identifier.endpage55en_US
dc.identifier.issn2148-4171
dc.identifier.issue1en_US
dc.identifier.startpage49en_US
dc.identifier.urihttps://www.hjse.hitit.edu.tr/hjse/index.php/HJSE/article/view/HJSE19030000077
dc.identifier.urihttps://hdl.handle.net/11491/430
dc.identifier.volume5en_US
dc.indekslendigikaynakTR-Dizin
dc.language.isoen
dc.publisherHitit University
dc.relation.ispartofHittite Journal of Science and Engineering
dc.relation.publicationcategoryMakale - Ulusal Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/openAccess
dc.subjectLiFePO4en_US
dc.subjectLithium Ion Batteryen_US
dc.subjectMechanochemical Activationen_US
dc.subjectNb Dopingen_US
dc.titleSynthesis, characterization and electrochemical performance of Nb doped LiFePO4/C cathodes by mechanochemical activation
dc.typeArticle

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