Optimization of the schiff-base reaction of acetylacetone with biogenic amines

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Tarih

2017

Dergi Başlığı

Dergi ISSN

Cilt Başlığı

Yayıncı

Hitit University

Erişim Hakkı

info:eu-repo/semantics/openAccess

Özet

In this work, optimum conditions for the derivatization reaction of biogenic amines (histamine, tyramine, putrecine, tryptamine, phenylethylamine, cadaverine, spermidine and spermine) with acetylacetone have been determined. In this reaction, the amount of K2HPO4, reaction time, reagent amount, solvent choice and solvent amount were optimized. As a result of this study, optimum conditions were determined as amount of K2HPO4 2 g, reaction time 20 min, amount of acetylacetone 1 mL, solvent methanol and amount of solvent 10 mL.

Açıklama

Anahtar Kelimeler

Biogenic Amines, Acetylacetone, Derivatization, Schiff Base

Kaynak

Hittite Journal of Science and Engineering

WoS Q Değeri

Scopus Q Değeri

Cilt

4

Sayı

1

Künye

Akmeşe, B., Asan, A.(2017). Optimization of the schiff-base reaction of acetylacetone with biogenic amines. Hittite Journal of Science and Engineering, 4(1), 79-83.