Single step calciothermic synthesis of nickel boride particles in molten salt

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dc.authorid0000-0002-6291-8947
dc.contributor.authorKartal, Levent
dc.date.accessioned2023-05-30T11:13:42Z
dc.date.available2023-05-30T11:13:42Z
dc.date.issued2023en_US
dc.departmentHitit Üniversitesi, Mühendislik Fakültesi, Metalurji ve Malzeme Mühendisliği Bölümü
dc.description.abstractAbstract In this study, production of nickel boride (NixB) via calciothermic reduction in molten salt has been studied. Firstly, the electrochemical behaviors of CaO and NiO in CaCl2 melt were examined by cyclic voltammetry (CV). Then, the influences of the process parameters (temperature (1173–1273 K) and time (15–60 min)) on the powders were investigated. Based on the CV results, it was understood that NiO reduction takes place in one step at -0.25 V. Temperature investigations revealed that Ni and Ni2B phases that were present at low temperatures disappeared as the temperature increased. The Ni3B and Ni2B ratios in the particles increased as the duration went on, and almost no Ni left in the particles after 60 min. The magnetic properties of the particles were investigated and, the saturation magnetization, coercive and remanent values were determined as 25.063 emu/g, 32.694 Oe, and 0.903 emu/g, respectively. © 2023, The Author(s) under exclusive licence to Australian Ceramic Society.
dc.description.provenanceSubmitted by Zeynep Umut NARİN (umutarslan@hitit.edu.tr) on 2023-05-30T11:09:12Z No. of bitstreams: 0en
dc.description.provenanceApproved for entry into archive by Zeynep Umut NARİN (umutarslan@hitit.edu.tr) on 2023-05-30T11:13:42Z (GMT) No. of bitstreams: 0en
dc.description.provenanceMade available in DSpace on 2023-05-30T11:13:42Z (GMT). No. of bitstreams: 0 Previous issue date: 2023en
dc.identifier.citationKartal, L. (2023). Single step calciothermic synthesis of nickel boride particles in molten salt. Journal of the Australian Ceramic Society, 1-10.
dc.identifier.doi10.1007/s41779-023-00893-9
dc.identifier.issn2510-1560
dc.identifier.scopusqualityQ2
dc.identifier.urihttps://doi.org/10.1007/s41779-023-00893-9
dc.identifier.urihttps://hdl.handle.net/11491/8478
dc.identifier.wosWOS:000990422900001
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringer
dc.relation.ispartofJournal of the Australian Ceramic Society
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/openAccess
dc.subjectMolten salt electrolysisen_US
dc.subjectCalciothermic reductionen_US
dc.subjectBoride particlesen_US
dc.subjectNickel borideen_US
dc.subjectNickelen_US
dc.titleSingle step calciothermic synthesis of nickel boride particles in molten salt
dc.typeArticle

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