Platinized carbon nanoelectrodes as potentiometric and amperometric SECM probes
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Tarih
2013
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Erişim Hakkı
info:eu-repo/semantics/closedAccess
Özet
Micrometer-sized platinized carbon electrodes have previously been used for the detection of reactive oxygen and nitrogen species (ROS and RNS) in biological systems. Here, we report the preparation and characterization of quartz-sealed platinized carbon nanoelectrodes. Such electrodes can be employed as tips in the scanning electrochemical microscope (SECM). The prepared electrodes were characterized by steady-state voltammetry, scanning electron microscopy, and SECM. In addition to ROS/RNS detection, the high surface area of a platinized nanoelectrode makes it a useful potentiometric probe. Unlike previously fabricated platinized electrodes, carbon electrodes possess a very thin insulating sheath, which is essential for experiments inside biological cells and high-resolution SECM imaging. © Springer-Verlag Berlin Heidelberg 2013.
Açıklama
Anahtar Kelimeler
Electrochemistry, Platinized Carbon Nanoelectrode, Potentiometry, Scanning Electrochemical Microscopy
Kaynak
Journal of Solid State Electrochemistry
WoS Q Değeri
N/A
Scopus Q Değeri
Q2
Cilt
17
Sayı
12
Künye
Hu, K., Gao, Y., Wang, Y., Yu, Y., Zhao, X., Rotenberg, S. A., ... & Gogotsi, Y. (2013). Platinized carbon nanoelectrodes as potentiometric and amperometric SECM probes. Journal of Solid State Electrochemistry, 17(12), 2971-2977.