Synthesis, spectroscopic studies and electrochemical properties of Schiff bases derived from 5-chloro-2-hydroxybenzaldehyde with methyl 2-amino-6-methyl-4,5,6,7-tetrahydrobenzo[b] thiophene-3-carboxylate

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dc.authoridKaya, Kerem / 0000-0002-5736-488X
dc.authorwosidKaya, Kerem / V-3794-2017
dc.contributor.authorColak, N.
dc.contributor.authorGunduzalp, A. B.
dc.contributor.authorMamas, S.
dc.contributor.authorAkkaya, D.
dc.contributor.authorKaya, K.
dc.date.accessioned2021-11-01T14:58:19Z
dc.date.available2021-11-01T14:58:19Z
dc.date.issued2016
dc.department[Belirlenecek]
dc.description.abstractSchiff base; methyl 2-((5-chloro-2-hydroxybenzylidene) amino)-6-methyl-4,5,6,7-tetrahydrothieno[ 2,3-c] pyridine-3-carboxylate was synthesized by the reaction of methyl 2-amino-6-methyl-4,5,6,7-tetrahydrothieno[2,3-c] pyridine-3-carboxylate with 5-chloro-2-hydroxybenzaldehyde in excellent yield. This compound was characterized by elemental analysis, NMR (H-1 and C-13-APT), FT-IR and X-ray diffraction methods. The electrochemical behavior of Schiff base was investigated using cyclic voltammetry (CV), controlled potential electrolysis and chronoamperometry (CA) techniques. The number of electrons transferred (n), diffusion coefficient (D) and standard heterogeneous rate constants (k(s)) were also determined by electrochemical methods.
dc.description.sponsorshipHitit UniversityHitit University [FEF19004.13.001]en_US
dc.description.sponsorshipWe thank for financially supported by Hitit University (No. FEF19004.13.001).en_US
dc.identifier.endpage26en_US
dc.identifier.issn0324-1130
dc.identifier.startpage20en_US
dc.identifier.urihttps://hdl.handle.net/11491/6590
dc.identifier.volume48en_US
dc.identifier.wosWOS:000392342400005
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.institutionauthor[Belirlenecek]
dc.language.isoen
dc.publisherBulgarian Acad Science
dc.relation.ispartofBulgarian Chemical Communications
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectSchiff baseen_US
dc.subject2-aminothiopheneen_US
dc.subjectX-ray diffractionen_US
dc.subjectelectrochemical behavioren_US
dc.titleSynthesis, spectroscopic studies and electrochemical properties of Schiff bases derived from 5-chloro-2-hydroxybenzaldehyde with methyl 2-amino-6-methyl-4,5,6,7-tetrahydrobenzo[b] thiophene-3-carboxylate
dc.typeArticle

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