Two novel mixed-ligand zinc-acesulfame compounds: Synthesis, spectroscopic and thermal characterization and biological applications

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dc.authorid0000-0001-9965-5573
dc.authorid0000-0003-4767-6799
dc.authorid0000-0003-4049-0756
dc.contributor.authorYurdakul, Ömer
dc.contributor.authorKöse, Dursun Ali
dc.contributor.authorŞahin, Onur
dc.contributor.authorAlp Avcı, Gülçin
dc.date.accessioned2020-01-30T13:57:08Z
dc.date.available2020-01-30T13:57:08Z
dc.date.issued2020en_US
dc.departmentHitit Üniversitesi, Fen Edebiyat Fakültesi, Kimya Bölümü
dc.description.abstractTwo new tetrahedral acesulfame complexes, acesulfamato(N)acesulfamato(O)bis(3-aminopyridine) zinc(II) (C18H20N6O8S2Zn, Zn-ace-3ap) and bis(acesulfamato-O)bis(benzotriazole)zinc(II) (C20H18N8O8S2Zn, Zn-ace-bta), were synthesized and characterized by single crystal X-ray diffraction, FT-IR spectroscopy, elemental analysis and thermal analysis techniques(TGA, DTA, DTG). The first compound, Zn-ace-3ap, crystallizes in triclinic space group P1 with parameters a?=?7.978 (7) Å, b?=?9.907 (6) Å, c?=?15.778 (14) Å, ??=?78.24° (2), ??=?81.22° (4), ??=?75.99° (2), Z?=?2 and The second compound, Zn-ace-bta, crystallizes in monoclinic space group C2/c with parameters a?=?19.879 (3) Å, b?=?9.3637 (13) Å, c?=?14.0852 (18) Å, ??=?105.483° (4), Z?=?4. The biological activities of the synthesized complexes were appraised through disk diffusion method as antibacterial, antimicrobial and antifungal in DMSO. Enterococcus faecalis (ATCC-29212), Staphylococcus aureus (ATCC-25923) as gram-positive bacteria, Pseudomonas aeroginosa (ATCC-27853) and Escherichia coli (ATCC-25922) as gram-negative bacteria, and Candida albicans (ATCC-10231) as fungus were grown with a view to investigate the antimicrobial effects of the complexes.
dc.description.provenanceSubmitted by Zeynep Umut Arslan (umutarslan@hitit.edu.tr) on 2020-01-30T13:56:48Z No. of bitstreams: 0en
dc.description.provenanceApproved for entry into archive by Zeynep Umut Arslan (umutarslan@hitit.edu.tr) on 2020-01-30T13:57:08Z (GMT) No. of bitstreams: 0en
dc.description.provenanceMade available in DSpace on 2020-01-30T13:57:08Z (GMT). No. of bitstreams: 0 Previous issue date: 2020en
dc.identifier.citationYurdakul, Ö., Köse, D. A., Şahin, O., Avcı, G. A. (2020). Two novel mixed-ligand zinc-acesulfame compounds: Synthesis, spectroscopic and thermal characterization and biological applications. Journal of Molecular Structure, 1203: 1-7.
dc.identifier.doi10.1016/j.molstruc.2019.127265
dc.identifier.endpage7en_US
dc.identifier.issn0022-2860
dc.identifier.scopusqualityQ1
dc.identifier.startpage1en_US
dc.identifier.urihttps://doi.org/10.1016/j.molstruc.2019.127265
dc.identifier.urihttps://hdl.handle.net/11491/5672
dc.identifier.volume1203en_US
dc.identifier.wosWOS:000504448700003
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherElsevier B.V.
dc.relation.ispartofJournal of Molecular Structure
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectAcesulfameen_US
dc.subjectBenzotriazoleen_US
dc.subjectBiological Applicationsen_US
dc.subject3-Aminopyridineen_US
dc.titleTwo novel mixed-ligand zinc-acesulfame compounds: Synthesis, spectroscopic and thermal characterization and biological applications
dc.typeArticle

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