Electrochemical Glucose Detection Using PdAg Nanoparticles Anchored on rGO/MWCNT Nanohybrids

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dc.authoridGökmeşe, Ebru / 0000-0002-5807-3494
dc.contributor.authorUzunoğlu, Aytekin
dc.contributor.authorKöse, Dursun Ali
dc.contributor.authorGökmeşe, Ebru
dc.contributor.authorGökmeşe, Faruk
dc.date.accessioned2021-11-01T15:03:15Z
dc.date.available2021-11-01T15:03:15Z
dc.date.issued2020
dc.departmentHitit Üniversitesi, Fen Edebiyat Fakültesi, Kimya Bölümü
dc.description.abstractThe combination of multi-walled carbon nanotube (MWCNT) and graphene (Gr) to extend their unique physicochemical properties to 3-dimensions (3D) is known to be an effective way to achieve high catalytic properties in electrochemistry. In this context, PdAg metal nanoparticles (MNPs) were anchored on 3-D MWCNT-rGO nanohybrids to construct high-performance enzyme-free electrochemical glucose sensors. The PdAg/MWCNT-rGO nanohybrids were prepared via a one-pot synthesis route and characterized using X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), thermogravimetric analysis (TGA), and X-ray photoelectron spectroscopy (XPS) methods. The XRD and TEM results confirmed the successful immobilization of PdAg nanoparticles on the support surface and the EDS results revealed a homogeneous MNP distribution. The PdAg content anchored on the hybrids was found to be 39 wt% by TGA analysis, which is compatible with the starting stoichiometric ratio. The constructed sensors showed the sensitivities of 13.16 +/- 0.4 and 5.22 +/- 0.07 mu A mM(-1) cm(-2) in the concentration windows of 0.05 to 4 and 4 to 42 mM, respectively. A wide linear range of 0.05 to 42 mM with a low limit of detection (51 mu M) was obtained from the sensors.
dc.identifier.citationElectrochemical Glucose Detection Using PdAg Nanoparticles Anchored on rGO/MWCNT Nanohybrids
dc.identifier.doi10.1007/s10876-019-01641-5
dc.identifier.endpage239en_US
dc.identifier.issn1040-7278
dc.identifier.issn1572-8862
dc.identifier.issue1en_US
dc.identifier.scopus2-s2.0-85069495529
dc.identifier.scopusqualityQ1
dc.identifier.startpage231en_US
dc.identifier.urihttps://doi.org/10.1007/s10876-019-01641-5
dc.identifier.urihttps://hdl.handle.net/11491/7046
dc.identifier.volume31en_US
dc.identifier.wosWOS:000513242600020
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthorKöse, Dursun Ali
dc.institutionauthorGökmeşe, Ebru
dc.institutionauthorGökmeşe, Faruk
dc.language.isoen
dc.publisherSpringer/Plenum Publishers
dc.relation.ispartofJournal Of Cluster Science
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectElectrochemical sensoren_US
dc.subjectGlucoseen_US
dc.subjectGrapheneen_US
dc.subjectMulti Walled Carbon Nanotubeen_US
dc.subjectPalladiumen_US
dc.subjectSilveren_US
dc.titleElectrochemical Glucose Detection Using PdAg Nanoparticles Anchored on rGO/MWCNT Nanohybrids
dc.typeArticle

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